Course Title: Inorganic Quantitative Analysis
Type of Course: Compulsory, Sessional, Non-departmental
Offered to: EEE
Pre-requisite Course(s): None
Volumetric analysis: Acidimetry-Alkalimetry. Titrations involving redox reactions: Determination of Fe, Cu, and Ca volumetrically. Determination of Ca and Mg in water.
To develop the basic understanding of a student dealing with chemical reagents, equipment necessary to perform quantitative inorganic analysis along with associated theoretical knowledge on acidimetry-alkalimetry, redox and complexometry
To provide hands on experience on the techniques of volumetric methods in analyte determination and to prepare students presenting their experimental findings as scientific reports
N/A
CO Statement Upon successful completion of the course, students should be able to: |
Corresponding PO(s)* | Domains and Taxonomy level(s)** | Delivery Method(s) and Activity(-ies) | Assessment Tool(s) | |
|---|---|---|---|---|---|
| CO1 | Describe different parameters and techniques related to inorganic quantitative analysis | PO(a) | C1 | Lectures | Quiz, Class performance, viva, Report writing |
| CO2 | Follow the instructions to perform guided enquiry in determining volume of titrants in different kinds of titrations | PO(d), PO(i) | P3 | Lectures and Demonstration | Quiz, Class performance, viva, Report writing Final Exam |
| CO3 | Analyze the experimental data for quantitative estimation of an analyte individually or by a group | PO(b), PO(i) | C4 | Lectures, Demonstration | Quiz, Class performanc, viva, Report writing Final Exam |
| CO4 | Prepare scientific reports on experiments by organizing experimental findings | PO(l) | C6 | Homework | Quiz, Class performanc, viva, Report writing, Final Exam |
Cognitive Domain Taxonomy Levels: C1 – Knowledge, C2 – Comprehension, C3 – Application, C4 – Analysis, C5 – Synthesis, C6 – Evaluation, Affective Domain Taxonomy Levels: A1: Receive; A2: Respond; A3: Value (demonstrate); A4: Organize; A5: Characterize; Psychomotor Domain Taxonomy Levels: P1: Perception; P2: Set; P3: Guided Response; P4: Mechanism; P5: Complex Overt Response; P6: Adaptation; P7: Organization
Program Outcomes (PO): PO(a) Engineering Knowledge, PO(b) Problem Analysis, PO(c) Design/development Solution, PO(d) Investigation,
PO(e) Modern tool usage, PO(f) The Engineer and Society, PO(g) Environment and sustainability, PO(h) Ethics, PO(i) Individual work and team work,
PO(j). Communication, PO(k) Project management and finance, PO(l) Life-long Learning
* For details of program outcome (PO) statements, please see the departmental website or course curriculum
| K1 | K2 | K3 | K4 | K5 | K6 | K7 | K8 | P1 | P2 | P3 | P4 | P5 | P6 | P7 | A1 | A2 | A3 | A4 | A5 |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Lecture Topics | References | Corresponding CO(s) | |
|---|---|---|---|
| L1 | Briefing on lab safety protocol and quiz on it | CO1 | |
| L2 | Course outline and introductory discussions on chemical analysis | CO1 | |
| Standardization of NaOH solution with standard oxalic acid solution | CO1 - CO4 | ||
| L4 | Standardization of hydrochloric acid with standard NaOH solution | CO1 - CO4 | |
| L5 | Standardization of HCl with standard Na2CO3 solution | CO1 - CO4 | |
| L6 | Standardization of sodium thiosulphate solution with a standard potassium dichromate solution | CO1 - CO4 | |
| L7 | Estimation of copper contained in a supplied solution by iodometric method | CO1 - CO4 | |
| L8 | Determination of ferrous iron by a standard potassium dichromate solution | CO1 - CO4 | |
| L9 | Standardization of potassium permanganate solution with standard sodium oxalate solution | CO1 - CO4 | |
| L10 | Determination of ferrous ion in a solution by standard KMnO4 solution | CO1 - CO4 | |
| L11 | Determination of calcium in a sample of calcium carbonate | CO1 - CO4 | |
| L12 | Viva | CO1, CO3 | |
| L13 | Practical exam | CO2, CO3 | |
| L14 | Quiz | CO1, CO3 |
Class Participation: Class participation and attendance will be recorded in every class.
Continuous Assessment: Continuous assessment will be accomplished following any of the activities such as quizzes, report writing and viva. The scheme of the continuous assessment for the course will be declared on the first day of classes
Final Examination: Practical examination will be held individually at the end of the sessional classes.
Attendance and Class Performance 20
Report 30
Quiz 40
Viva 20
Final Examination 40
Total 150
Quantitative Inorganic Analysis, By: A. I. Vogel